1-[1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl]-1-ethanone

Base Information

• Chemical Name: 1-[1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl]-1-ethanone
• CAS No.: 1033463-42-1
• Molecular Formula: C₁₂H₁₂ClN₃O
• Molecular Weight: 249.7
• Mol file: 1033463-42-1.mol

Synonyms:1-(1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl)ethanone

Chemical Property of 1-[1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl]-1-ethanone

Chemical Property:

• Melting Point: 98°

Purity/Quality:

98%min ^*data from raw suppliers

1-[1-(4-Chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl]-1-ethanone >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 1-[1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl]-1-ethanone

There total 1 articles about 1-[1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl]-1-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

para-Chlorobenzyl alcohol (873-76-7) + acetylacetone (123-54-6,81235-32-7) → 1-(1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl)ethanone (1033463-42-1)

Guidance literature:

para-Chlorobenzyl alcohol; With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3.15h; Inert atmosphere;

acetylacetone; In N,N-dimethyl-formamide; at 60 - 70 ℃; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.tetlet.2014.12.019

Reference yield: 52.0%

1-(1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl)ethanone (1033463-42-1) + 5,11,17,23-tetra-tert-butyl-25,27-di(ethoxycarbonylmethoxy)-26,28-dihydroxycalix[4]arene (1262336-92-4,97600-49-2) → C72H80Cl2N6O8 (1529759-94-1)

Guidance literature:

1-(1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl)ethanone; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.166667h;

5,11,17,23-tetra-tert-butyl-25,27-di(ethoxycarbonylmethoxy)-26,28-dihydroxycalix[4]arene; In tetrahydrofuran; mineral oil; at 0 ℃; for 1.5h; Reflux;

DOI:10.1016/j.cclet.2014.03.012

Reference yield: 36.0%

1-(1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl)ethanone (1033463-42-1) + 25,27-bis[(ethoxycarbonyl)methoxy]-26,28-dihydroxycalix[4]arene (142267-55-8) → C56H48Cl2N6O8 (1529759-98-5)

Guidance literature:

1-(1-(4-chlorobenzyl)-5-methyl-1H-1,2,3-triazol-4-yl)ethanone; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.166667h;

25,27-bis[(ethoxycarbonyl)methoxy]-26,28-dihydroxycalix[4]arene; In tetrahydrofuran; mineral oil; at 0 ℃; for 1.5h; Reflux;

DOI:10.1016/j.cclet.2014.03.012

upstream raw materials:

para-Chlorobenzyl alcohol

acetylacetone

Downstream raw materials:

C₇₂H₈₀Cl₂N₆O₈

C₅₆H₄₈Cl₂N₆O₈

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