2-(p-cyanophenyl)-3-phenylindene

Base Information

• Chemical Name: 2-(p-cyanophenyl)-3-phenylindene
• CAS No.: 52033-65-5
• Molecular Formula: C₂₂H₁₅N
• Molecular Weight: 293.368
• Mol file: 52033-65-5.mol

Synonyms:2-(p-cyanophenyl)-3-phenylindene

Chemical Property of 2-(p-cyanophenyl)-3-phenylindene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(p-cyanophenyl)-3-phenylindene

There total 7 articles about 2-(p-cyanophenyl)-3-phenylindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

1-(p-cyanophenyl)-1-phenylindene (52033-62-2) → 2-phenyl-3-(p-cyanophenyl)indene (52033-68-8) + 2-(p-cyanophenyl)-3-phenylindene (52033-65-5)

Guidance literature:

In hexane; for 0.183333h; Product distribution; Quantum yield; Irradiation; other solvents, other temperature, sensitizer, thermolysis, 14C isotope experiment;

DOI:10.1021/jo00318a018

Reference yield:

phthalic anhydride (85-44-9) → 2-(p-cyanophenyl)-3-phenylindene (52033-65-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 80 percent / sodium acetate / 2 h / 230 - 240 °C

2: 39 percent / diethyl ether; benzene / Heating

3: 58 mg / zinc, mercuric chloride / aq. ethanol; aq. HCl / 4 h / Heating

4: 42 percent / zinc, mercuric chloride, conc. HCl / various solvent(s) / 2 h / Heating

With hydrogenchloride; sodium acetate; mercury dichloride; zinc; In hydrogenchloride; diethyl ether; ethanol; benzene;

DOI:10.1021/jo00318a018

Reference yield:

1-(p-cyanophenyl)-1-phenylindene (52033-62-2) → 2-(p-cyanophenyl)-3-phenylindene (52033-65-5)

Guidance literature:

In diphenylether; Heating;

DOI:10.1021/ja00813a066

upstream raw materials:

1-(p-cyanophenyl)-1-phenylindene

4-(1-oxo-3-phenyl-1H-inden-2-yl)benzonitrile

phthalic anhydride

(Z)-3-(4-bromobenzylidene)isobenzofuran-1(3H)-one