C₂₃H₁₅F₃N₂O₅

Base Information

Chemical Name:C₂₃H₁₅F₃N₂O₅
CAS No.:1037763-61-3
Molecular Formula:C₂₃H₁₅F₃N₂O₅
Molecular Weight:456.378
Hs Code.:

C<sub>23</sub>H<sub>15</sub>F<sub>3</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₃H₁₅F₃N₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₁₅F₃N₂O₅

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Technology Process of C₂₃H₁₅F₃N₂O₅

There total 8 articles about C₂₃H₁₅F₃N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1037763-59-9
C₂₅H₁₉F₃N₂O₅

: 1037763-61-3
C₂₃H₁₅F₃N₂O₅

Guidance literature:: C₂₅H₁₉F₃N₂O₅; With methanol; lithium hydroxide; water; at 120 ℃; for 0.333333h; Microwave irradiation;

With hydrogenchloride; water; pH=1;

Reference yield:

: 1544-85-0
2,2-difluoro-benzo[1,3]dioxol-5-ylamine

: 1037763-61-3
C₂₃H₁₅F₃N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: bromine; acetic acid / 1 h / 20 °C

2.1: hydrogenchloride; acetic acid; tin(ll) chloride / 0.5 h / 110 - 115 °C

3.1: N-Methyldicyclohexylamine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine / 1,4-dioxane / 18 h / 100 °C

4.1: N-iodo-succinimide / acetone / 3 h / 20 °C

5.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 3.5 h / 90 °C

6.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

7.1: methanol; lithium hydroxide; water / 0.33 h / 120 °C / Microwave irradiation

7.2: pH 1

With hydrogenchloride; methanol; lithium hydroxide; N-iodo-succinimide; N-Methyldicyclohexylamine; water; bromine; potassium carbonate; caesium carbonate; acetic acid; tin(ll) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1037763-50-0
C₇H₄BrF₂NO₂

: 1037763-61-3
C₂₃H₁₅F₃N₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Methyldicyclohexylamine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine / 1,4-dioxane / 18 h / 100 °C

2.1: N-iodo-succinimide / acetone / 3 h / 20 °C

3.1: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 3.5 h / 90 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

5.1: methanol; lithium hydroxide; water / 0.33 h / 120 °C / Microwave irradiation

5.2: pH 1

With methanol; lithium hydroxide; N-iodo-succinimide; N-Methyldicyclohexylamine; water; potassium carbonate; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetone;