C₂₁H₃₀O₃Si

Base Information

Chemical Name:C₂₁H₃₀O₃Si
CAS No.:1424338-07-7
Molecular Formula:C₂₁H₃₀O₃Si
Molecular Weight:358.553
Hs Code.:

C<sub>21</sub>H<sub>30</sub>O<sub>3</sub>Si

Synonyms:C₂₁H₃₀O₃Si

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Chemical Property of C₂₁H₃₀O₃Si

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Technology Process of C₂₁H₃₀O₃Si

There total 4 articles about C₂₁H₃₀O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1424338-05-5
C₂₁H₂₈O₄Si

: 1424338-07-7
C₂₁H₃₀O₃Si

Guidance literature:: With aluminum (III) chloride; sodium tetrahydroborate; In diethyl ether; for 4h; Reflux;
DOI:10.1016/j.tetlet.2013.01.040

Reference yield:

: 1424338-04-4
C₁₄H₂₄O₃Si

: 1424338-07-7
C₂₁H₃₀O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 4 h / 0 - 5 °C

2: aluminum (III) chloride; sodium tetrahydroborate / diethyl ether / 4 h / Reflux

With aluminum (III) chloride; sodium tetrahydroborate; In diethyl ether; dichloromethane; 1: |Friedel-Crafts Acylation;
DOI:10.1016/j.tetlet.2013.01.040

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1424338-07-7
C₂₁H₃₀O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1H-imidazole / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

2: aluminum (III) chloride / dichloromethane / 4 h / 0 - 5 °C

3: aluminum (III) chloride; sodium tetrahydroborate / diethyl ether / 4 h / Reflux

With 1H-imidazole; dmap; aluminum (III) chloride; sodium tetrahydroborate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; 2: |Friedel-Crafts Acylation;
DOI:10.1016/j.tetlet.2013.01.040