Technology Process of C56H64BF2N7O7
There total 8 articles about C56H64BF2N7O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; copper; sodium L-ascorbate;
In
tetrahydrofuran; water;
at 70 ℃;
for 6h;
Inert atmosphere;
DOI:10.1016/j.tet.2013.03.082
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone
2.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
2.2: 0.33 h / 0 - 20 °C / Inert atmosphere
2.3: 0 - 20 °C / Inert atmosphere
3.1: piperidine; acetic acid / toluene / Reflux; Dean-Stark
4.1: copper; copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 6 h / 70 °C / Inert atmosphere
With
piperidine; copper(ll) sulfate pentahydrate; copper; potassium carbonate; acetic acid; sodium L-ascorbate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; acetone; toluene;
3.1: |Knoevenagel Condensation;
DOI:10.1016/j.tet.2013.03.082
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
1.2: 0.33 h / 0 - 20 °C / Inert atmosphere
1.3: 0 - 20 °C / Inert atmosphere
2.1: piperidine; acetic acid / toluene / Reflux; Dean-Stark
3.1: copper; copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 6 h / 70 °C / Inert atmosphere
With
piperidine; copper(ll) sulfate pentahydrate; copper; acetic acid; sodium L-ascorbate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; toluene;
2.1: |Knoevenagel Condensation;
DOI:10.1016/j.tet.2013.03.082
