2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide

Base Information

• Chemical Name: 2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide
• CAS No.: 1245567-43-4
• Molecular Formula: C₁₄H₁₅N₅O₂
• Molecular Weight: 285.305
• Mol file: 1245567-43-4.mol

Synonyms:2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide

Chemical Property of 2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide

There total 1 articles about 2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-{[4-(methoxycarbonyl)phenyl]amino}benzoic acid methyl ester → 2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide (1245567-43-4)

Guidance literature:

With hydrazine hydrate; for 6h; Reflux;

DOI:10.1016/j.ejmech.2010.05.072

Reference yield: 95.0%

carbon disulfide (75-15-0,12122-00-8) + 2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide (1245567-43-4) → 4-amino-5-{2-[4-(4-amino-5-mercapto-4H-1,2,4-triazol-3-yl)phenylamino]phenyl}-4H-1,2,4-triazole-3-thiol (1245567-48-9)

Guidance literature:

carbon disulfide; 2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide; With potassium hydroxide; In ethanol; at 20 ℃; Cooling with ice;

With hydrazine hydrate; In diethyl ether; ethanol; water; for 2h; Reflux;

DOI:10.1016/j.ejmech.2010.05.072

Reference yield: 95.0%

2-[4-(hydrazinecarbonyl)phenylamino]benzoic acid hydrazide (1245567-43-4) + benzaldehyde (100-52-7) → 2,4'-azanediylbis(N'-benzylidenebenzohydrazide) (1245567-44-5)

Guidance literature:

With acetic acid; In ethanol; for 4h; Reflux;

DOI:10.1016/j.ejmech.2010.05.072

Downstream raw materials:

2,4'-azanediylbis[N'-(furan-2-ylmethylene)benzohydrazide]

4-amino-5-{2-[4-(4-amino-5-mercapto-4H-1,2,4-triazol-3-yl)phenylamino]phenyl}-4H-1,2,4-triazole-3-thiol

5-{2-[4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenylamino]phenyl}-1,3,4-oxadiazole-2-thiol

2,4'-azanediylbis{N'-[(5-nitrofuran-2-yl)methylene]benzohydrazide}