Technology Process of C54H71N5O10
There total 7 articles about C54H71N5O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 6h;
Inert atmosphere;
Reflux;
DOI:10.1039/b9nj00305c
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium carbonate / acetonitrile / 1 h / 80 °C / Inert atmosphere
1.2: 17 h / 70 °C / Inert atmosphere
2.1: trifluoro-[1,3,5]triazine; pyridine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 61.5 h / 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere; Reflux
5.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / -60 - -30 °C / Inert atmosphere
6.1: aminosulfonic acid; sodium chlorite / tetrahydrofuran; water / 13 h / 20 °C / Inert atmosphere
7.1: dicyclohexyl-carbodiimide; dmap; benzotriazol-1-ol / dichloromethane / 60 h / 20 °C / Inert atmosphere
8.1: trifluoroacetic acid / dichloromethane / 6 h / Inert atmosphere; Reflux
With
pyridine; dmap; sodium chlorite; trifluoro-[1,3,5]triazine; oxalyl dichloride; aminosulfonic acid; tetrabutyl ammonium fluoride; potassium carbonate; benzotriazol-1-ol; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: trifluoro-[1,3,5]triazine; pyridine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 61.5 h / 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere; Reflux
4: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / -60 - -30 °C / Inert atmosphere
5: aminosulfonic acid; sodium chlorite / tetrahydrofuran; water / 13 h / 20 °C / Inert atmosphere
6: dicyclohexyl-carbodiimide; dmap; benzotriazol-1-ol / dichloromethane / 60 h / 20 °C / Inert atmosphere
7: trifluoroacetic acid / dichloromethane / 6 h / Inert atmosphere; Reflux
With
pyridine; dmap; sodium chlorite; trifluoro-[1,3,5]triazine; oxalyl dichloride; aminosulfonic acid; tetrabutyl ammonium fluoride; benzotriazol-1-ol; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water;