hydroxy-3 phenyl-2 pentene-2 dithioate de methyle

Base Information

Chemical Name:hydroxy-3 phenyl-2 pentene-2 dithioate de methyle
CAS No.:126557-99-1
Molecular Formula:C₁₂H₁₄OS₂
Molecular Weight:238.375
Hs Code.:

Synonyms:hydroxy-3 phenyl-2 pentene-2 dithioate de methyle

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hydroxy-3 phenyl-2 pentene-2 dithioate de methyle

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Technology Process of hydroxy-3 phenyl-2 pentene-2 dithioate de methyle

There total 2 articles about hydroxy-3 phenyl-2 pentene-2 dithioate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 126557-90-2,126558-08-5
hydroxy-3 phenyl-2 pentanedithioate de methyle

: 126557-99-1
hydroxy-3 phenyl-2 pentene-2 dithioate de methyle

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; 1.) - 50 deg C, 20 min: 2.) - 50 deg C, 20 min: 3.) -40 deg C, 5 min; 25 deg C, 10 min;

Reference yield:

: 2168-85-6
methyl phenyldithioacetate

: 126557-99-1
hydroxy-3 phenyl-2 pentene-2 dithioate de methyle

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / 1.) LDA / tetrahydrofuran / 1.) -78 deg C, 30 min; 2.) 3 min

2: 90 percent / 1.) oxalyl chloride, dimethylsulfoxyde; 3.) triethylamine / CH₂Cl₂ / 1.) - 50 deg C, 20 min: 2.) - 50 deg C, 20 min: 3.) -40 deg C, 5 min; 25 deg C, 10 min

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;