(E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide

Base Information

Chemical Name:(E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide
CAS No.:1581720-66-2
Molecular Formula:Br*C₂₀H₂₃N₂O₅
Molecular Weight:451.317
Hs Code.:

Synonyms:(E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide

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Chemical Property of (E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide

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Technology Process of (E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide

There total 2 articles about (E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 19199-82-7
4-nitrophenyl 2-bromoacetate

: (E)-1-bromo-3-(p-methoxyphenyl)-1-propene

: 1581720-66-2
(E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide

Guidance literature:: In diethyl ether; dichloromethane; at 20 - 25 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja500758n

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1581720-66-2
(E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / ethyl acetate / 2.17 h / 0 - 25 °C / Inert atmosphere

2: diethyl ether; dichloromethane / 16 h / 20 - 25 °C / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/ja500758n

Reference yield: 60.0%

: 1581720-66-2
(E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide

: 100-46-9
benzylamine

: 1581720-26-4
(2S,3S)-N-benzyl-2-(dimethylamino)-3-(4-methoxyphenyl)pent-4-enamide

Guidance literature:: (E)-3-(4-methoxyphenyl)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)prop-2-en-1-aminium bromide; With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; benzotriazol-1-ol; diisopropylamine; In acetonitrile; at -20 ℃; for 24h; Inert atmosphere;

benzylamine; In acetonitrile; at 20 - 25 ℃; for 24h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja500758n