threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline

Base Information

Chemical Name:threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline
CAS No.:78739-31-8
Molecular Formula:C₂₅H₃₉NO₂
Molecular Weight:385.59
Hs Code.:

threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ<sup>2</sup>-oxazoline

Synonyms:threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline

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Chemical Property of threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline

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Technology Process of threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline

There total 8 articles about threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2-phenyl-4-(S)-[(4S,5S)-4-(tetradecyl)-1,3,2-dioxathiolane-2,2-dioxide-5-yl]-1,3-oxazoline

: 78739-31-8,161968-12-3
threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline

Guidance literature:: 2-phenyl-4-(S)-[(4S,5S)-4-(tetradecyl)-1,3,2-dioxathiolane-2,2-dioxide-5-yl]-1,3-oxazoline; With tetra-(n-butyl)ammonium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 70 ℃; for 5h; Reflux;

With sulfuric acid; water; In tetrahydrofuran; methanol; at 22 ℃; for 3h;
DOI:10.1002/ejoc.201100911

Reference yield:

: 78715-83-0
methyl (S)-2-phenyl-4,5-dihydrooxazole-4-carboxylate

: 78739-31-8,161968-12-3
threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline

Guidance literature:: Multi-step reaction with 2 steps

1: DIBAL-H / hexane; toluene / 3 h / -70 °C

2: 1.) DIBAL-H / 2.) ether, toluene, warming from 5 to 23 deg C, 1 h

With diisobutylaluminium hydride; In hexane; toluene;
DOI:10.1021/jo00335a015

Reference yield:

: 825-60-5
benzimidic acid ethyl ester

: 78739-31-8,161968-12-3
threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ²-oxazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / CH₂Cl₂; H₂O / 16 h

2: DIBAL-H / hexane; toluene / 3 h / -70 °C

3: 1.) DIBAL-H / 2.) ether, toluene, warming from 5 to 23 deg C, 1 h

With diisobutylaluminium hydride; In hexane; dichloromethane; water; toluene;
DOI:10.1021/jo00335a015