di-i-butylammonium tetrafluoroborate

Base Information

• Chemical Name: di-i-butylammonium tetrafluoroborate
• CAS No.: 17251-80-8
• Molecular Formula: BF₄*C₈H₁₉N*H
• Molecular Weight: 217.058

Synonyms:di-i-butylammonium tetrafluoroborate

Chemical Property of di-i-butylammonium tetrafluoroborate

Chemical Property:

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Technology Process of di-i-butylammonium tetrafluoroborate

There total 1 articles about di-i-butylammonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Di-sec-butylamin (626-23-3) + pyridinium tetrafluoroborate → pyridine (110-86-1) + di-i-butylammonium tetrafluoroborate (17251-80-8)

Guidance literature:

In water; taking C5H5NHBF4 in a beaker, cooling in an ice-bath, dropwise addn. of the amine, exothermic react., stirring the soln. at 0 - 5°C (30 min); extn. of pyridine with ether, pptn., filtration on suction, washing with ether until free from pyridine, drying over P2O5, elem. anal.;

upstream raw materials:

Di-sec-butylamin

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