5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde

Base Information

Chemical Name:5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde
CAS No.:1429318-59-1
Molecular Formula:C₃₉H₄₃NOS₂
Molecular Weight:605.909
Hs Code.:

Synonyms:5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde

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Chemical Property of 5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde

Chemical Property:

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Technology Process of 5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde

There total 3 articles about 5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1259331-94-6
5’-bromo-3,4’-dihexyl-2,2’-bithiophene-5-aldehyde

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1429318-59-1
5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In toluene; for 16h; Reflux; Inert atmosphere;
DOI:10.3762/bjoc.9.122

Reference yield:

: 748763-44-2
(4-hexylthiophen-2-yl)boronic acid

: 1429318-59-1
5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; tetrahydrofuran / Inert atmosphere; Reflux

2: acetic acid; N-Bromosuccinimide / chloroform / 0 - 20 °C / Inert atmosphere; Darkness

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; tetrahydrofuran / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; acetic acid; In tetrahydrofuran; chloroform; water;
DOI:10.1039/c5tc03308j

Reference yield:

: 291535-21-2
4-hexyl-5-bromo-2-thiophenecarboxaldehyde

: 1429318-59-1
5'-(4-(diphenylamino)phenyl)-3,4'-dihexyl-[2,2'-bithiophene]-5-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; tetrahydrofuran / Inert atmosphere; Reflux

2: acetic acid; N-Bromosuccinimide / chloroform / 0 - 20 °C / Inert atmosphere; Darkness

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; tetrahydrofuran / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; acetic acid; In tetrahydrofuran; chloroform; water;
DOI:10.1039/c5tc03308j