4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

Base Information

Chemical Name:4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one
CAS No.:1417802-02-8
Molecular Formula:C₃₁H₃₀O₇
Molecular Weight:514.575
Hs Code.:

Synonyms:4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

Suppliers and Price of 4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

There total 17 articles about 4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417802-01-7
6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-ol

: 129660-02-2
4-chloro-2(H)-pyran-2-one

: 1417802-02-8
4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

Guidance literature:: With potassium carbonate; In acetonitrile; at 70 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol303390a

Reference yield:

: 1417801-99-0
C₂₂H₃₉BO₄Si

: 1417802-02-8
4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium bromide / 1,4-dioxane / 36 h / 80 °C / Inert atmosphere

2: boron trichloride; dichloromethane / dichloromethane / 0.5 h / -78 - -30 °C / Inert atmosphere

3: potassium carbonate / acetonitrile / 12 h / 70 °C / Inert atmosphere

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloromethane; water; boron trichloride; potassium carbonate; potassium bromide; In 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1021/ol303390a

Reference yield:

: 1417801-87-6
5'-(benzyloxy)-2-isopropoxy-3,4'-dimethoxy-2',6-divinyl-1,1'-biphenyl

: 1417802-02-8
4-((6-(2-(3-hydroxypropyl)-4-methoxyphenyl)-3,7-dimethoxy-9,10-dihydrophenanthren-4-yl)oxy)-2H-pyran-2-one

Guidance literature:: Multi-step reaction with 6 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 22 h / 50 °C / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 24 h / 31029.7 Torr / Inert atmosphere

3: pyridine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

4: water; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium bromide / 1,4-dioxane / 36 h / 80 °C / Inert atmosphere

5: boron trichloride; dichloromethane / dichloromethane / 0.5 h / -78 - -30 °C / Inert atmosphere

6: potassium carbonate / acetonitrile / 12 h / 70 °C / Inert atmosphere

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloromethane; 5%-palladium/activated carbon; water; hydrogen; boron trichloride; potassium carbonate; potassium bromide; In 1,4-dioxane; dichloromethane; ethyl acetate; acetonitrile; 1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol303390a