((C₄H₂NC(p-MeC₆H₄))4)CoBr

Base Information

Chemical Name:((C₄H₂NC(p-MeC₆H₄))4)CoBr
CAS No.:34829-90-8
Molecular Formula:C₄₈H₃₆BrCoN₄
Molecular Weight:807.738
Hs Code.:

((C<sub>4</sub>H<sub>2</sub>NC(p-MeC<sub>6</sub>H<sub>4</sub>))4)CoBr

Synonyms:((C₄H₂NC(p-MeC₆H₄))4)CoBr

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Chemical Property of ((C₄H₂NC(p-MeC₆H₄))4)CoBr

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Technology Process of ((C₄H₂NC(p-MeC₆H₄))4)CoBr

There total 1 articles about ((C₄H₂NC(p-MeC₆H₄))4)CoBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 19414-65-4
meso-tetratolylporphyrinatocobalt(II)

: 10035-10-6,12258-64-9
hydrogen bromide

: 34829-90-8
((C₄H₂NC(p-MeC₆H₄))4)CoBr

Guidance literature:: In methanol; chloroform; water; addn. of aq. HBr to CHCl3:MeOH soln. of Co-complex, stirring at room temp. for 2 h; NMR spectroscopy;
DOI:10.1021/om9705315

Reference yield: 73.0%

: 680-31-9
N,N,N,N,N,N-hexamethylphosphoric triamide

: 34829-90-8
((C₄H₂NC(p-MeC₆H₄))4)CoBr

: 19414-65-4
meso-tetratolylporphyrinatocobalt(II)

: ((C₄H₂NC(p-MeC₆H₄))4)Co(PO(NMe₂)2)

Guidance literature:: With 1,1,1,2,2,2-hexamethyldisilane; methyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N2-atmosphere; addn. of MeLi (ether) to soln. of disilane (HMPA) at 0°C, stirring for 15 min, addn. of THF, cooling (-78°C), addn.of soln. of Co-complex (THF), warming to 0°C for 1 h; chromy. (SiO2); elem. anal.;
DOI:10.1021/om9705315

Reference yield: 38.0%

: 34829-90-8
((C₄H₂NC(p-MeC₆H₄))4)CoBr

: 1605-65-8
N,N,N',N'-Tetramethylphosphorodiamidic chloride

: 19414-65-4
meso-tetratolylporphyrinatocobalt(II)

: ((C₄H₂NC(p-MeC₆H₄))4)Co(PO(NMe₂)2)

Guidance literature:: With potassium; In tetrahydrofuran; N2-atmosphere; addn. of (Me2N)2(O)PCl to suspension of K, stirring for 24 h at room temp., cooling (-78°C), addn. of soln. of Co-complex,warming to 0°C; pouring into pentane, washing (H2O), drying (MgSO4), evapn., chromy. (SiO2, CH2Cl2, CH2Cl2:MeOH 95:5), evapn.;
DOI:10.1021/om9705315