11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester

Base Information

• Chemical Name: 11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester
• CAS No.: 1000174-37-7
• Molecular Formula: C₂₅H₃₈O₄
• Molecular Weight: 402.574
• Mol file: 1000174-37-7.mol

Synonyms:11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester

Chemical Property of 11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester

There total 1 articles about 11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

11-[3-(5-tert-butyldimethylsilanyloxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester (1000174-36-6) → 11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester (1000174-37-7)

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran;

DOI:10.1016/j.bmc.2007.08.039

Reference yield: 88.0%

11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester (1000174-37-7) → 11-[3-(5-bromo-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester (1000174-39-9)

Guidance literature:

With carbon tetrabromide; TOP; In diethyl ether; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2007.08.039

Reference yield:

11-[3-(5-hydroxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester (1000174-37-7) + methanesulfonyl chloride (124-63-0) → C26H40O6S

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2007.08.039

upstream raw materials:

11-[3-(5-tert-butyldimethylsilanyloxy-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester

Downstream raw materials:

11-[3-(5-bromo-1,1-dimethylpentyl)phenoxy]undeca-5,8-dienoic acid methyl ester