11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Base Information

Chemical Name:11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate
CAS No.:1408287-76-2
Molecular Formula:C₃₀H₃₀N₂O₆
Molecular Weight:514.578
Hs Code.:

Synonyms:11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

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Chemical Property of 11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

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Technology Process of 11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

There total 5 articles about 11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1421916-41-7
11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

: 1408287-76-2
11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 0 ℃;
DOI:10.2533/chimia.2013.213

Reference yield:

: 1408287-78-4
C₂₄H₃₄N₂O₉

: 1408287-76-2
11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 20 °C

3: lithium hydroxide; water / tetrahydrofuran / 0 °C

With hydrogenchloride; water; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.2533/chimia.2013.213

Reference yield:

: 1027338-06-2
4-dibenzocyclooctynol

: 1408287-76-2
11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 8 h / 25 °C

2: triethylamine / N,N-dimethyl-formamide / 20 °C

3: lithium hydroxide; water / tetrahydrofuran / 0 °C

With pyridine; water; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.2533/chimia.2013.213