11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Base Information

Chemical Name:11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate
CAS No.:1421916-41-7
Molecular Formula:C₃₆H₃₆N₂O₉
Molecular Weight:640.69
Hs Code.:

Synonyms:11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

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Chemical Property of 11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

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Technology Process of 11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

There total 5 articles about 11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1027338-09-5
11,12-didehydro-5,6-dihydrodibenzo[a,e]cycloocten-5-yl carbonic acid 4-nitrophenyl ester

: 1408287-73-9
5-[(6-aminohexyl)carbamoyl]benzene-1,2,3-triyl triacetate

: 1421916-41-7
11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.2533/chimia.2013.213

Reference yield:

: 1027338-06-2
4-dibenzocyclooctynol

: 1421916-41-7
11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 8 h / 25 °C

2: triethylamine / N,N-dimethyl-formamide / 20 °C

With pyridine; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.2533/chimia.2013.213

Reference yield:

: 6635-24-1
3,4,5-triacetoxybenzoic acid

: 1421916-41-7
11,12-didehydro-5,6-dihydrodibenzo[a,e][8]annulen-5-yl (6-{[(3,4,5-trihydroxyphenyl)carbonyl]amino}hexyl) carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1.25 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.25 h / 0 - 20 °C

3: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

4: triethylamine / N,N-dimethyl-formamide / 20 °C

With hydrogenchloride; oxalyl dichloride; triethylamine; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.2533/chimia.2013.213