(-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

Base Information

Chemical Name:(-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene
CAS No.:130353-27-4
Molecular Formula:C₁₆H₂₀O₄
Molecular Weight:276.332
Hs Code.:

Synonyms:(-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

Suppliers and Price of (-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

There total 4 articles about (-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109715-12-0
2,3-O-Isopropyliden-2-C-methyl-5-O-p-toluolsulfonyl-D-ribo-pentonsaeure-γ-lacton

: 130353-27-4
(-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / NaI / butan-2-one / 3 h / Heating

2: 95 percent / Zn, HOAc / H₂O; tetrahydrofuran / 3 h / Ambient temperature

3: diethyl ether

4: 98 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

5: 95 percent / pyridine / 1 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; acetic acid; sodium iodide; zinc; In tetrahydrofuran; diethyl ether; water; butanone;
DOI:10.1021/jo00001a073

Reference yield:

: 130353-10-5
(+)-(2R,3R)-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-enoic acid

: 130353-27-4
(-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: 98 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

3: 95 percent / pyridine / 1 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00001a073

Reference yield:

: 85963-85-5
(-)-(2R,3R)-methyl 2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-enoate

: 130353-27-4
(-)-(2S,3R)-1-O-benzoyl-2,3-dihydroxy-2,3-O-isopropylidene-2-methylpent-4-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

2: 95 percent / pyridine / 1 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo00001a073