10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one

Base Information

Chemical Name:10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one
CAS No.:130888-44-7
Molecular Formula:C₂₂H₁₈N₂O₃S
Molecular Weight:390.463
Hs Code.:

Synonyms:10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one

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Chemical Property of 10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one

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Technology Process of 10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one

There total 15 articles about 10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 104587-06-6
7-oxo-8-phenyl-7H-thieno<2,3-a>quinolizine-10-carboxylic acid

: 104604-13-9
8-oxo-9-phenyl-4,5,6,8-tetrahydro-pyrido[1,2-a]thieno[2,3-c]azepin-11-carboxylic acid

: 130888-44-7
10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one

Guidance literature:: With thionyl chloride; In 1,4-dioxane; N-methyl-acetamide; toluene;

Reference yield:

: 28948-58-5
7-chlorothieno<2,3-c>pyridine

: 130888-44-7
10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / NaHS*H₂O / dimethylformamide / 3 h / 110 - 115 °C

2: 2) NEt₃ / 1) CH₂Cl₂, 45 min

3: 87 percent / toluene / 8 h / Heating

4: 94 percent / NaOH / methanol; H₂O / 24 h / Heating

5: SOCl₂ / 1 h / Ambient temperature

6: NEt₃ / toluene / Ambient temperature

With sodium hydroxide; sodium hydrogensulfide; thionyl chloride; triethylamine; In methanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19900730402

Reference yield:

: 104587-44-2
thieno<2,3-c>pyridine-7(6H)-thione

: 130888-44-7
10-<(morpholin-4-yl)carbonyl>-8-phenyl-7H-thieno<2,3-a>quinolizin-7-one

Guidance literature:: Multi-step reaction with 5 steps

1: 2) NEt₃ / 1) CH₂Cl₂, 45 min

2: 87 percent / toluene / 8 h / Heating

3: 94 percent / NaOH / methanol; H₂O / 24 h / Heating

4: SOCl₂ / 1 h / Ambient temperature

5: NEt₃ / toluene / Ambient temperature

With sodium hydroxide; thionyl chloride; triethylamine; In methanol; water; toluene;
DOI:10.1002/hlca.19900730402