methyl 3-hydroxy-2-(1-methylpiperidine-2-carboxamido)benzoate

Base Information

• Chemical Name: methyl 3-hydroxy-2-(1-methylpiperidine-2-carboxamido)benzoate
• CAS No.: 1006601-60-0
• Molecular Formula: C₁₅H₂₀N₂O₄
• Molecular Weight: 292.335
• Mol file: 1006601-60-0.mol

Synonyms:methyl 3-hydroxy-2-(1-methylpiperidine-2-carboxamido)benzoate

Chemical Property of methyl 3-hydroxy-2-(1-methylpiperidine-2-carboxamido)benzoate

Chemical Property:

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Technology Process of methyl 3-hydroxy-2-(1-methylpiperidine-2-carboxamido)benzoate

There total 1 articles about methyl 3-hydroxy-2-(1-methylpiperidine-2-carboxamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-3-hydroxy-benzoic acid methyl ester (17672-21-8) + 1-methylpiperidine-2-carboxylic acid hydrochloride (25271-35-6) → 2-amino-3-(methoxycarbonyl)phenyl 1-methylpiperidine-2-carboxylate (1006601-58-6) + methyl 3-hydroxy-2-(1-methylpiperidine-2-carboxamido)benzoate (1006601-60-0)

Guidance literature:

2-amino-3-hydroxy-benzoic acid methyl ester; 1-methylpiperidine-2-carboxylic acid hydrochloride; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 17h;

upstream raw materials:

2-amino-3-hydroxy-benzoic acid methyl ester

1-methylpiperidine-2-carboxylic acid hydrochloride