N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine

Base Information

Chemical Name:N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine
CAS No.:713519-83-6
Molecular Formula:C₃₀H₃₅N₅O₅
Molecular Weight:545.638
Hs Code.:

Synonyms:N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine

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Chemical Property of N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine

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Technology Process of N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine

There total 4 articles about N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 713519-55-2
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

: 713519-83-6
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine

Guidance literature:: With sodium hydroxide; water; In 1,4-dioxane; at 0 ℃; for 6h;
DOI:10.1002/ejoc.200300692

Reference yield:

: 14338-36-4
3-amino phenylacetic acid

: 713519-83-6
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; HCl / H₂O / 0.33 h

1.2: 98 percent / H₂O; acetic acid / 2 h / 20 °C

2.1: 70 percent / DCC; HOBt / dimethylformamide

3.1: 98 percent / NaOH; water / dioxane / 6 h / 0 °C

With hydrogenchloride; sodium hydroxide; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200300692

Reference yield:

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 713519-83-6
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; HCl / H₂O / 0.33 h

1.2: 98 percent / H₂O; acetic acid / 2 h / 20 °C

2.1: 70 percent / DCC; HOBt / dimethylformamide

3.1: 98 percent / NaOH; water / dioxane / 6 h / 0 °C

With hydrogenchloride; sodium hydroxide; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200300692