N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester
CAS No.:713519-55-2
Molecular Formula:C₃₁H₃₇N₅O₅
Molecular Weight:559.665
Hs Code.:

Synonyms:N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

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Chemical Property of N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

There total 3 articles about N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 26348-68-5
N-(benzyloxycarbonyl)lysine methyl ester hydrochloride

: 386207-00-7
3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetic acid

: 713519-55-2
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200300692

Reference yield:

: 14338-36-4
3-amino phenylacetic acid

: 713519-55-2
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; HCl / H₂O / 0.33 h

1.2: 98 percent / H₂O; acetic acid / 2 h / 20 °C

2.1: 70 percent / DCC; HOBt / dimethylformamide

With hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200300692

Reference yield:

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 713519-55-2
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]phenylacetyl}lysine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; HCl / H₂O / 0.33 h

1.2: 98 percent / H₂O; acetic acid / 2 h / 20 °C

2.1: 70 percent / DCC; HOBt / dimethylformamide

With hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200300692