6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol

Base Information

Chemical Name:6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol
CAS No.:579494-03-4
Molecular Formula:C₆₅H₇₀O₁₂
Molecular Weight:1043.26
Hs Code.:

Synonyms:6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol

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Chemical Property of 6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol

Chemical Property:

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Technology Process of 6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol

There total 7 articles about 6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2R,3S,4S,5R,6R)-2-[(1R,2R,3S,4S,5R,6S)-3-allyloxy-4,5,6-tris-benzyloxy-2-(4-methoxy-benzyloxy)-cyclohexyloxy]-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl ester

: 579494-03-4
6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol

Guidance literature:: With methylamine; In ethanol; at 20 ℃; for 6h;
DOI:10.1016/j.carres.2003.06.002

Reference yield:

: 100-39-0
benzyl bromide

: 579494-03-4
6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 84 percent / sodium hydride / dimethylformamide / 4 h / 20 °C

2.1: 95 percent / camphor-10-sulfonic acid / CH₂Cl₂; methanol / 24 h / 20 °C

3.1: dibutyltin oxide / toluene / 3 h / Heating

3.2: 79 percent / tetrabutylammonium iodide / toluene / 1.5 h / 110 °C

4.1: trimethylsilyl triflate / diethyl ether / 0 h / 20 °C

5.1: methylamine / ethanol / 6 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; sodium hydride; di(n-butyl)tin oxide; methylamine; In methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2003.06.002

Reference yield:

: 131233-71-1,1214020-75-3
1D-4-O-allyl-1,5,6-tri-O-benzyl-myo-inositol

: 579494-03-4
6-O-allyl-3,4,5-tri-O-benzyl-1-O-(4-methoxybenzyl)-2-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-L-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1.1: dibutyltin oxide / toluene / 3 h / Heating

1.2: 79 percent / tetrabutylammonium iodide / toluene / 1.5 h / 110 °C

2.1: trimethylsilyl triflate / diethyl ether / 0 h / 20 °C

3.1: methylamine / ethanol / 6 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; di(n-butyl)tin oxide; methylamine; In diethyl ether; ethanol; toluene;
DOI:10.1016/j.carres.2003.06.002