2-Methyl-3-phenyl-2,3-dihydro-1-benzofuran

Base Information

Chemical Name:2-Methyl-3-phenyl-2,3-dihydro-1-benzofuran
CAS No.:51677-43-1
Molecular Formula:C₁₅H₁₄O
Molecular Weight:210.276
Hs Code.:
NSC Number:87375
DSSTox Substance ID:DTXSID90965957

Synonyms:51677-43-1;2-methyl-3-phenyl-2,3-dihydro-1-benzofuran;NSC87375;DTXSID90965957;NSC-87375;3-phenyl-2-methyl-dihydro-benzofuran

Suppliers and Price of 2-Methyl-3-phenyl-2,3-dihydro-1-benzofuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Methyl-3-phenyl-2,3-dihydro-1-benzofuran

Chemical Property:

Vapor Pressure:0.00212mmHg at 25°C
Boiling Point:299.4°C at 760 mmHg
Flash Point:130.2°C
Density:1.085g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:210.104465066
Heavy Atom Count:16
Complexity:232

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C(C2=CC=CC=C2O1)C3=CC=CC=C3

Technology Process of 2-Methyl-3-phenyl-2,3-dihydro-1-benzofuran

There total 21 articles about 2-Methyl-3-phenyl-2,3-dihydro-1-benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38276-75-4
2-(1-phenylallyl)phenol

: 38281-39-9,38281-40-2,51677-43-1
trans-2-Methyl-3-phenyldihydrobenzofuran

: 38281-39-9,38281-40-2,51677-43-1
cis-2-Methyl-3-phenyldihydrobenzofuran

: C₁₅H₁₄O

: C₁₅H₁₄O

Guidance literature:: With titanium(IV) 2-ethylhexoxide; water; C₅₄H₆₈N₂O₁₀S₄; In cyclohexane; at 75 ℃; for 48h; Overall yield = 44 percent; enantioselective reaction; Inert atmosphere;
DOI:10.1021/acscatal.1c01146

Reference yield:

: 38276-75-4
2-(1-phenylallyl)phenol

: 38281-39-9,38281-40-2,51677-43-1
trans-2-Methyl-3-phenyldihydrobenzofuran

: 38281-39-9,38281-40-2,51677-43-1
cis-2-Methyl-3-phenyldihydrobenzofuran

: C₁₅H₁₄O

: C₁₅H₁₄O

Guidance literature:: With titanium(IV) 2-ethylhexoxide; water; C₅₄H₆₈N₂O₁₀S₄; In cyclohexane; at 75 ℃; for 48h; Overall yield = 44 percent; enantioselective reaction; Inert atmosphere;
DOI:10.1021/acscatal.1c01146

Reference yield:

: 117-99-7
2-Hydroxybenzophenone

: 38281-39-9,38281-40-2,51677-43-1
trans-2-methyl-3-phenyl-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 4 steps

1: 92.5 percent / NaOH / dimethylsulfoxide / 40 °C

2: 90.8 percent / hydrazine hydrate / ethanol / Heating

3: Na₂SO₄, yellow HgO, sat. ethanol. KOH / diethyl ether / 10 h / Ambient temperature

4: -196 °C / Irradiation

With potassium hydroxide; sodium hydroxide; hydrazine hydrate; sodium sulfate; mercury(II) oxide; In diethyl ether; ethanol; dimethyl sulfoxide;