2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole

Base Information

Chemical Name:2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole
CAS No.:1642145-27-4
Molecular Formula:C₂₂H₁₇N₅O
Molecular Weight:367.41
Hs Code.:

Synonyms:2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole

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Chemical Property of 2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole

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Technology Process of 2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole

There total 7 articles about 2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5651-86-5
4-(prop-2-ynyloxy)benzaldehyde

: 95-54-5
1,2-diamino-benzene

: 622-37-7
Phenyl azide

: 1642145-27-4
2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole

Guidance literature:: With alpha-D-glucopyranose; copper(ll) sulfate pentahydrate; In tetrahydrofuran; water; at 70 ℃; Solvent; Microwave irradiation;
DOI:10.3762/bjoc.10.145

Reference yield:

: 62-53-3
aniline

: 1642145-27-4
2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / 0 °C

1.2: 20 °C

2.1: copper(ll) sulfate pentahydrate; alpha-D-glucopyranose / tetrahydrofuran; water / 70 °C / Microwave irradiation

With hydrogenchloride; alpha-D-glucopyranose; copper(ll) sulfate pentahydrate; sodium nitrite; In tetrahydrofuran; water;
DOI:10.3762/bjoc.10.145

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1642145-27-4
2‐(4‐((1‐phenyl‐1H‐1,2,3‐triazol‐4‐yl)methoxy)phenyl)‐1H‐benzo[d]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: copper(ll) sulfate pentahydrate; alpha-D-glucopyranose / tetrahydrofuran; water / 70 °C / Microwave irradiation

With alpha-D-glucopyranose; copper(ll) sulfate pentahydrate; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.3762/bjoc.10.145