C₂₀H₂₅NO₆

Base Information

Chemical Name:C₂₀H₂₅NO₆
CAS No.:1351932-59-6
Molecular Formula:C₂₀H₂₅NO₆
Molecular Weight:375.422
Hs Code.:

C<sub>20</sub>H<sub>25</sub>NO<sub>6</sub>

Synonyms:C₂₀H₂₅NO₆

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Chemical Property of C₂₀H₂₅NO₆

Chemical Property:

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Technology Process of C₂₀H₂₅NO₆

There total 4 articles about C₂₀H₂₅NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1351932-58-5
C₂₇H₃₃NO₇

: 1351932-59-6
C₂₀H₂₅NO₆

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 50 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.10.042

Reference yield:

: C₁₉H₂₄INO₅

: 1351932-59-6
C₂₀H₂₅NO₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.10.042

Reference yield:

: 106221-07-2
(R)-1-((3aR,5R,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-prop-2-en-1-ol

: 1351932-59-6
C₂₀H₂₅NO₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethyl borane; oxygen / tetrahydrofuran; ethanol; water / 20 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 1.5 h / 0 - 20 °C / Inert atmosphere

3.2: 0.5 h / 20 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide / 5 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; triethyl borane; oxygen; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Kharash type reaction;
DOI:10.1016/j.tetlet.2011.10.042