di-t-butyl 2-(4,4,5,5-tetramethyl-1,3,2-di-oxaborolan-2-yl)isophthalate*2-hydroxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:di-t-butyl 2-(4,4,5,5-tetramethyl-1,3,2-di-oxaborolan-2-yl)isophthalate*2-hydroxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1253189-40-0
Molecular Formula:C₆H₁₃BO₃*C₂₂H₃₃BO₆
Molecular Weight:548.29
Hs Code.:

Synonyms:di-t-butyl 2-(4,4,5,5-tetramethyl-1,3,2-di-oxaborolan-2-yl)isophthalate*2-hydroxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-t-butyl 2-(4,4,5,5-tetramethyl-1,3,2-di-oxaborolan-2-yl)isophthalate*2-hydroxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of di-t-butyl 2-(4,4,5,5-tetramethyl-1,3,2-di-oxaborolan-2-yl)isophthalate*2-hydroxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about di-t-butyl 2-(4,4,5,5-tetramethyl-1,3,2-di-oxaborolan-2-yl)isophthalate*2-hydroxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1253189-33-1
di-tert-butyl 2-bromoisophthalate

: 1253189-40-0
di-t-butyl 2-(4,4,5,5-tetramethyl-1,3,2-di-oxaborolan-2-yl)isophthalate*2-hydroxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: di-tert-butyl 2-bromoisophthalate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 15h; Inert atmosphere;
DOI:10.1246/bcsj.20090342