N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

Base Information

Chemical Name:N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone
CAS No.:144709-18-2
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

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Technology Process of N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

There total 3 articles about N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 144709-27-3
3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

: 74-88-4
methyl iodide

: 144709-18-2
N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1h;
DOI:10.1016/S0040-4020(01)80496-8

Reference yield:

: 144709-15-9
[4,5-Dimethoxy-2-(1-oxo-1,2-dihydro-isoquinolin-3-yl)-phenyl]-acetic acid

: 74-88-4
methyl iodide

: 144709-18-2
N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1h; Yield given;
DOI:10.1016/S0040-4020(01)80496-8

Reference yield:

: 144709-15-9
[4,5-Dimethoxy-2-(1-oxo-1,2-dihydro-isoquinolin-3-yl)-phenyl]-acetic acid

: 144709-18-2
N-methyl-3-<2-(methoxycarbonylmethyl)-4,5-dimethoxyphenyl>-1(2H)-isoquinolone

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride etherate / 1 h / Heating

2: 88 percent / K₂CO₃ / dimethylformamide / 1 h / 80 °C

With boron trifluoride diethyl etherate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80496-8