Technology Process of C28H48O4Si
There total 12 articles about C28H48O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
dichloromethane;
at 20 ℃;
for 16h;
DOI:10.1039/b602020h
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 87 percent / pyridinium para-toluenesulfonate / methanol / 16 h / 25 °C
2.1: BF3*Et2O / CH2Cl2 / 6 h / -78 °C
3.1: O3 / CH2Cl2 / -78 °C
3.2: 90 percent / PPh3 / CH2Cl2 / 1 h / -78 - 25 °C
4.1: diethyl ether / 3 h / -78 °C
4.2: 2.95 g / aq. NaOH; H2O2 / diethyl ether; methanol / 16 h / 0 - 25 °C
5.1: 90 percent / imidazole / CH2Cl2 / 16 h / 20 °C
With
1H-imidazole; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; ozone;
In
methanol; diethyl ether; dichloromethane;
4.1: Brown allylation;
DOI:10.1039/b602020h
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 89 percent / DIBAL-H / toluene / 0.5 h / -78 °C
2.1: 87 percent / pyridinium para-toluenesulfonate / methanol / 16 h / 25 °C
3.1: BF3*Et2O / CH2Cl2 / 6 h / -78 °C
4.1: O3 / CH2Cl2 / -78 °C
4.2: 90 percent / PPh3 / CH2Cl2 / 1 h / -78 - 25 °C
5.1: diethyl ether / 3 h / -78 °C
5.2: 2.95 g / aq. NaOH; H2O2 / diethyl ether; methanol / 16 h / 0 - 25 °C
6.1: 90 percent / imidazole / CH2Cl2 / 16 h / 20 °C
With
1H-imidazole; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; ozone;
In
methanol; diethyl ether; dichloromethane; toluene;
5.1: Brown allylation;
DOI:10.1039/b602020h
