Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester

Base Information

• Chemical Name: Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester
• CAS No.: 173034-47-4
• Molecular Formula: C₂₆H₂₆Cl₂NO₅P
• Molecular Weight: 534.376
• Mol file: 173034-47-4.mol

Synonyms:Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester

Chemical Property of Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester

There total 7 articles about Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

6-(6-Chloro-9-methyl-acridin-2-yloxy)-hexan-1-ol (173034-40-7) + 2-chlorophenyl dichlorophosphate (15074-54-1) → Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester (173034-47-4)

Guidance literature:

In pyridine; at -10 ℃;

DOI:10.1002/hlca.19980810528

Reference yield:

6-chloro-2-methoxy-9-methyl-acridine (22684-26-0) → Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester (173034-47-4)

Guidance literature:

Multi-step reaction with 4 steps

1: HBr / acetic acid; H₂O / 26 h / Heating

2: Cs₂CO₃ / dimethylformamide / 4 h / 120 °C

3: 96 percent / aq. HCl / ethanol / 1 h / Heating

4: 65 percent / pyridine / -10 °C

With hydrogenchloride; hydrogen bromide; caesium carbonate; In pyridine; ethanol; water; acetic acid; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19980810528

Reference yield:

6-Chloro-9-methyl-2-[6-(tetrahydro-pyran-2-yloxy)-hexyloxy]-acridine (210102-20-8) → Phosphoric acid 6-(6-chloro-9-methyl-acridin-2-yloxy)-hexyl ester 2-chloro-phenyl ester (173034-47-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / aq. HCl / ethanol / 1 h / Heating

2: 65 percent / pyridine / -10 °C

With hydrogenchloride; In pyridine; ethanol;

DOI:10.1002/hlca.19980810528

upstream raw materials:

6-(6-Chloro-9-methyl-acridin-2-yloxy)-hexan-1-ol

2-chlorophenyl dichlorophosphate

6-chloro-2-methoxy-9-methyl-acridine

6,9-dichloro-2-methoxyacridine