{2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene

Base Information

Chemical Name:{2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene
CAS No.:621110-87-0
Molecular Formula:C₃₀H₆₇Cl₂PSi₇
Molecular Weight:726.34
Hs Code.:

Synonyms:{2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene

Suppliers and Price of {2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene

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Technology Process of {2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene

There total 2 articles about {2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: (E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

: 621110-87-0
{2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene

Guidance literature:: (E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.5h;

With lithium chloride; phosphorus trichloride; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 16h;
DOI:10.1002/poc.608