2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine

Base Information

• Chemical Name: 2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine
• CAS No.: 882693-31-4
• Molecular Formula: C₃₀H₆₉PSi₇
• Molecular Weight: 657.45

Synonyms:2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine

Chemical Property of 2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine

Chemical Property:

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Technology Process of 2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine

There total 1 articles about 2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

{2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene (621110-87-0) → 2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine (882693-31-4)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1246/bcsj.80.1884

Reference yield: 81.0%

dichloro( 1,5-cyclooctadiene)platinum(ll) (12080-32-9) + 2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine (882693-31-4) → cis-[Cl2Pt(2,6-bis[trimethylsilyl)methyl]-4-[tri(trimethylsilyl)methyl]phenylphosphine)2] (1117894-61-7)

Guidance literature:

In chloroform; PtCl2(cod) and phosphine deriv. in CHCl3 at 72°C;

DOI:10.1246/cl.2008.1192

Reference yield: 77.0%

2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine (882693-31-4) + (9-anthracenyl)dichlorophosphane (141982-25-4) → BbtP=P(9-Anth) (1171247-70-3,1245629-83-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1246/bcsj.20090295

upstream raw materials:

{2,6-bis[(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl}dichlorophosphene

Downstream raw materials:

1,1'-bis[(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)PP]ferrocene

BbtP=P(9-Anth)

cis-[PtMe₂(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenylphosphine)2]

cis-[Cl₂Pt(2,6-bis[trimethylsilyl)methyl]-4-[tri(trimethylsilyl)methyl]phenylphosphine)2]

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