4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester

Base Information

Chemical Name:4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester
CAS No.:207125-61-9
Molecular Formula:C₁₈H₁₉NO₃
Molecular Weight:297.354
Hs Code.:

Synonyms:4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester

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Chemical Property of 4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester

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Technology Process of 4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester

There total 1 articles about 4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79328-86-2
1-(phenoxycarbonyl)-1,2-dihydropyridine

: 155930-86-2
4-diazo-5-hexen-3-one

: 207125-62-0
2-propionyl-6-aza-bicyclo[3.2.2]nona-2,8-diene-6-carboxylic acid phenyl ester

: 207125-61-9
4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester

Guidance literature:: rhodium(II) pivalate;
DOI:10.1021/jo0158940

Reference yield: 91.0%

: 207125-61-9
4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester

: 384842-98-2
4-propionyl-(6-phenoxycarbonyl-6-azabicyclo[3.2.2]non-3-ene)

Guidance literature:: With hydrogen; Wilkinson's catalyst; In ethanol; for 24h; under 2585.81 Torr;
DOI:10.1021/jo0158940

Reference yield:

: 207125-61-9
4-propionyl-6-aza-bicyclo[3.2.2]nona-3,8-diene-6-carboxylic acid phenyl ester

: 6-methyl-4β-propionyl-3β-p-tolyl-6-azabicyclo[3.2.2]nonane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 91 percent / H₂ / (PPh₃)3RhCl / ethanol / 24 h / 2585.81 Torr

2.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / Heating

3.1: 2.01 g / oxalyl chloride; DMSO / CH₂Cl₂ / 0.25 h / -78 °C

4.1: CuBr*SMe₂ / diethyl ether; tetrahydrofuran / 24 h / 0 - 20 °C

4.2: aq. HCl / tetrahydrofuran; diethyl ether / 23 °C

With lithium aluminium tetrahydride; oxalyl dichloride; copper(I) bromide dimethylsulfide complex; hydrogen; dimethyl sulfoxide; Wilkinson's catalyst; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo0158940