1(2H)-Pyridinecarboxylic acid, phenyl ester

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, phenyl ester
CAS No.:79328-86-2
Molecular Formula:C12H11NO2
Molecular Weight:201.225
Hs Code.:
DSSTox Substance ID:DTXSID10455022
Nikkaji Number:J953.008H
Wikidata:Q82276857

Synonyms:79328-86-2;1(2H)-Pyridinecarboxylic acid, phenyl ester;SCHEMBL3183679;DTXSID10455022;Phenyl pyridine-1(2H)-carboxylate;1,2-Dihydropyridine-1-carboxylic acid phenyl ester

Suppliers and Price of 1(2H)-Pyridinecarboxylic acid, phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1(2H)-Pyridinecarboxylic acid, phenyl ester

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:201.078978594
Heavy Atom Count:15
Complexity:277

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C=CC=CN1C(=O)OC2=CC=CC=C2

Technology Process of 1(2H)-Pyridinecarboxylic acid, phenyl ester

There total 7 articles about 1(2H)-Pyridinecarboxylic acid, phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110-86-1
pyridine

: 1885-14-9
phenyl chloroformate

: 79328-86-2
1-(phenoxycarbonyl)-1,2-dihydropyridine

Guidance literature:: pyridine; With sodium tetrahydroborate; In methanol; at -78 ℃;

phenyl chloroformate; In methanol; at -78 - -55 ℃; for 4h;
DOI:10.1021/jacs.5b08693

Reference yield:

: 110-86-1
pyridine

: 1885-14-9
phenyl chloroformate

: 79328-86-2
1-(phenoxycarbonyl)-1,2-dihydropyridine

: 90838-83-8
1-phenoxycarbonyl-1,4-dihydropyridine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 78 ℃; for 25h;
DOI:10.1016/j.tet.2010.07.026

Reference yield:

: 110-86-1
pyridine

: 79328-86-2
1-(phenoxycarbonyl)-1,2-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(I) iodide / tetrahydrofuran / 0.08 h

2: sodium borohydride

With sodium tetrahydroborate; copper(l) iodide; In tetrahydrofuran;
DOI:10.1021/jo970039v