2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol

Base Information

• Chemical Name: 2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol
• CAS No.: 757244-92-1
• Molecular Formula: C₂₃H₃₂O₂S
• Molecular Weight: 372.572

Synonyms:2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol

Chemical Property of 2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol

There total 1 articles about 2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-tert-butyl-6-mercapto-4-methylphenol (38146-04-2) + 2-bromomethyl-6-tert-butyl-4-methylphenol → 2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol (757244-92-1)

Guidance literature:

With potassium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 14.5h;

Reference yield: 100.0%

2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol (757244-92-1) + titanium tetrachloride (7550-45-0) → dichloro{1-monothiaethanediyl-2,2'-bis(6-tert-butyl-4-methylphenolate)}titanium

Guidance literature:

In dichloromethane; at 0 - 20 ℃; for 0.5h;

Reference yield: 96.0%

2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol (757244-92-1) + tetrabenzyl titanium (17520-19-3) → dibenzyl{1-monothiaethanediyl-2,2'-bis-(6-tert-butyl-4-methylphenolate)-}titanium

Guidance literature:

In pentane; at -30 - 20 ℃; for 2h;

upstream raw materials:

2-tert-butyl-6-mercapto-4-methylphenol

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