2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester

Base Information

Chemical Name:2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester
CAS No.:118469-71-9
Molecular Formula:C₂₈H₄₈BrO₇P
Molecular Weight:607.563
Hs Code.:

Synonyms:2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester

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Chemical Property of 2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester

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Technology Process of 2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester

There total 3 articles about 2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74597-04-9
m-hydroxybenzyl bromide

: 118469-71-9
2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / POCl₃, Et₃N / CCl₄ / 20 h / 25 °C

2: Et₃N / CCl₄ / 2 h / 25 °C

3: 0.5 M NaOAc / tetrahydrofuran / 24 h

With sodium acetate; triethylamine; trichlorophosphate; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jm00153a005

Reference yield:

: Acetic acid 2-[(3-bromomethyl-phenoxy)-chloro-phosphoryloxy]-1-hexadecyloxymethyl-ethyl ester

: 118469-71-9
2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester

Guidance literature:: With sodium acetate; In tetrahydrofuran; for 24h; Yield given;
DOI:10.1021/jm00153a005

Reference yield:

: 99884-78-3
3-(bromomethyl)phenyl phosphodichlorodate

: 118469-71-9
2-(acetyloxy)-3-(hexadecyloxy)propyl 3-(bromomethyl)phenyl phosphoric acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CCl₄ / 2 h / 25 °C

2: 0.5 M NaOAc / tetrahydrofuran / 24 h

With sodium acetate; triethylamine; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jm00153a005