7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Base Information

Chemical Name:7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal
CAS No.:156336-34-4
Molecular Formula:C₂₃H₃₄O₂
Molecular Weight:342.522
Hs Code.:

Synonyms:7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Suppliers and Price of 7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

There total 4 articles about 7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: (2E,4E,6E)-3-Methyl-7-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-undeca-2,4,6-triene-1,11-diol

: 156336-34-4
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 36h; Ambient temperature;

Reference yield:

: 56013-01-5
triphenyl((2,6,6-trimethylcyclohex-1-enyl)methyl)phosphonium bromide

: 156336-34-4
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, RT, 0.5 h, 2.) THF, hexane, from -78 deg C to RT, 12 h

2: n-Bu₄NF / tetrahydrofuran / 2 h / Ambient temperature

3: 27 percent / MnO₂ / CH₂Cl₂ / 36 h / Ambient temperature

With manganese(IV) oxide; n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 156336-33-3
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

: 156336-34-4
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Guidance literature:: Multi-step reaction with 2 steps

1: n-Bu₄NF / tetrahydrofuran / 2 h / Ambient temperature

2: 27 percent / MnO₂ / CH₂Cl₂ / 36 h / Ambient temperature

With manganese(IV) oxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;