7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

Base Information

Chemical Name:7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether
CAS No.:156336-33-3
Molecular Formula:C₂₉H₅₀O₂Si
Molecular Weight:458.8
Hs Code.:

Synonyms:7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

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Chemical Property of 7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

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Technology Process of 7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

There total 1 articles about 7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56013-01-5
triphenyl((2,6,6-trimethylcyclohex-1-enyl)methyl)phosphonium bromide

: 2-(4'-hydroxybutyl)-6-methyl-8-<(tert-butyldimethylsilyl)oxy>-2,4,6-octatrienal

: 156336-33-3
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

Guidance literature:: With n-butyllithium; Multistep reaction; 1.) THF, hexane, RT, 0.5 h, 2.) THF, hexane, from -78 deg C to RT, 12 h;

Reference yield:

: 156336-33-3
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

: (2E,4E,6E)-3-Methyl-7-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-undeca-2,4,6-triene-1,11-diol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

: 156336-33-3
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenyl tert-butyldimethylsilyl ether

: 156336-34-4
7-(4'-hydroxybutyl)-9-(2',6',6'-trimethyl-1'-cyclohexenyl)-3-methyl-2,4,6,8-nonatetraenal

Guidance literature:: Multi-step reaction with 2 steps

1: n-Bu₄NF / tetrahydrofuran / 2 h / Ambient temperature

2: 27 percent / MnO₂ / CH₂Cl₂ / 36 h / Ambient temperature

With manganese(IV) oxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;