Technology Process of C40H47N9O2
There total 7 articles about C40H47N9O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; L-ascorbic acid sodium;
In
tetrahydrofuran; water;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1002/anie.201105375
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / 24 h / Reflux; Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 0 - 20 °C
3.1: methanol / 24 h / Reflux
3.2: 24 h / 0 - 20 °C
4.1: copper(ll) sulfate pentahydrate; L-ascorbic acid sodium / tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; copper(ll) sulfate pentahydrate; L-ascorbic acid sodium; potassium carbonate;
In
tetrahydrofuran; methanol; water; acetone;
DOI:10.1002/anie.201105375
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / methanol / 24 h / Reflux
1.2: 24 h / 0 °C
2.1: hydrogenchloride / methanol; water
2.2: 24 h / 80 °C
3.1: copper(ll) sulfate pentahydrate; L-ascorbic acid sodium / tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere
With
hydrogenchloride; copper(ll) sulfate pentahydrate; L-ascorbic acid sodium; triethylamine;
In
tetrahydrofuran; methanol; water;
DOI:10.1002/anie.201105375