2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide

Base Information

• Chemical Name: 2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide
• CAS No.: 1094165-00-0
• Molecular Formula: C₃₅H₃₈N₂O₈S₂
• Molecular Weight: 678.827

Synonyms:2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide

Chemical Property of 2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide

Chemical Property:

Purity/Quality:

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Technology Process of 2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide

There total 1 articles about 2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.3%

methylphenylsulfonate (3112-85-4) + N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl (1094164-87-0) → 2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide (1094165-00-0)

Guidance literature:

methylphenylsulfonate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With water; acetic acid; In tetrahydrofuran;

DOI:10.1021/jo802410u

Reference yield: 82.3%

2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide (1094165-00-0) + 2-(2-methoxyethoxy)ethyl iodide (104539-21-1) → 2-benzenesulfonyl-N-{5-{[2-benzenesulfonyl-4-(2-methoxyethoxy)butyryl]benzyloxyamino}pentyl}-N-benzyloxy-4-(2-ethoxyethoxy)butyramide (1094165-05-5)

Guidance literature:

With potassium carbonate; In acetonitrile; for 96h; Reflux;

DOI:10.1021/jo802410u

upstream raw materials:

methylphenylsulfonate

N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

Downstream raw materials:

2-benzenesulfonyl-N-{5-{[2-benzenesulfonyl-4-(2-methoxyethoxy)butyryl]benzyloxyamino}pentyl}-N-benzyloxy-4-(2-ethoxyethoxy)butyramide

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