N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

Base Information

Chemical Name:N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl
CAS No.:1094164-87-0
Molecular Formula:C₂₅H₃₄N₂O₆
Molecular Weight:458.555
Hs Code.:

Synonyms:N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

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Chemical Property of N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

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Technology Process of N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

There total 1 articles about N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 5555-72-6
N-benzyloxycarbamic acid ethyl ester

: 1094164-87-0
N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 48h;
DOI:10.1021/jo802410u

Reference yield: 84.0%

: 540-88-5
acetic acid tert-butyl ester

: 1094164-87-0
N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

: 1094164-99-4
N-benzyloxy-N-[5-(benzyloxy-tert-butoxycarbonylacetylamino)pentyl]malonamic acid tert-butyl ester

Guidance literature:: acetic acid tert-butyl ester; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With water; acetic acid; In tetrahydrofuran;
DOI:10.1021/jo802410u

Reference yield: 77.3%

: 3112-85-4
methylphenylsulfonate

: 1094164-87-0
N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl

: 1094165-00-0
2-benzenesulfonyl-N-[5-(N-(benzenesulfonylacetyl)-N-benzyloxy-amino)pentyl]-N-benzyloxy acetamide

Guidance literature:: methylphenylsulfonate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N-benzyloxy-[5-(benzyloxyethoxycarbonylamino)pentyl]carbamic acid ethyl; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With water; acetic acid; In tetrahydrofuran;
DOI:10.1021/jo802410u