1-PROPIOPHENONE TOSYLHYDRAZONE 97

Base Information

Chemical Name:1-PROPIOPHENONE TOSYLHYDRAZONE 97
CAS No.:17336-66-2
Molecular Formula:C16H18N2O2S
Molecular Weight:302.397
Hs Code.:2935009090
DSSTox Substance ID:DTXSID80938372
ChEMBL ID:CHEMBL2132364
Mol file:17336-66-2.mol

Synonyms:1-PROPIOPHENONE TOSYLHYDRAZONE 97;PROPIOPHENONE (P-TOSYL)HYDRAZONE;1-propiophenone p-toluenesulfonylhydrazone;

Suppliers and Price of 1-PROPIOPHENONE TOSYLHYDRAZONE 97

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
PROPIOPHENONE (P-TOSYL)HYDRAZONE Aldrich
1ea
$ 57.00

Sigma-Aldrich
1-Propiophenone tosylhydrazone 97%
25g
$ 187.00

American Custom Chemicals Corporation
1-PROPIOPHENONE TOSYLHYDRAZONE 95.00%
25G
$ 1289.16

Alfa Aesar
Propionophenone p-toluenesulfonylhydrazone, 97%
25g
$ 150.00

Alfa Aesar
Propionophenone p-toluenesulfonylhydrazone, 97%
5g
$ 40.20

Total 11 raw suppliers

Chemical Property of 1-PROPIOPHENONE TOSYLHYDRAZONE 97

Chemical Property:

Melting Point:118-120oC(lit.)
Boiling Point:448.4±38.0 °C(Predicted)
PKA:9.81±0.40(Predicted)
Flash Point:225oC
PSA：66.91000
Density:1.15±0.1 g/cm3(Predicted)
LogP:4.55930
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:302.10889899
Heavy Atom Count:21
Complexity:439

Purity/Quality:

95% ^*data from raw suppliers

PROPIOPHENONE (P-TOSYL)HYDRAZONE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=NNS(=O)(=O)C1=CC=C(C=C1)C)C2=CC=CC=C2

Technology Process of 1-PROPIOPHENONE TOSYLHYDRAZONE 97

There total 2 articles about 1-PROPIOPHENONE TOSYLHYDRAZONE 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 93-55-0
1-phenyl-propan-1-one

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 17336-66-2
propiophenone N-tosylhydrazone

Guidance literature:: In methanol; at 60 ℃; for 4h;

Reference yield:

: 17336-66-2
propiophenone N-tosylhydrazone

Guidance literature:: DOI:10.1055/s-1976-24109 DOI:10.1021/jo01038a515

Reference yield: 100.0%

: 67853-37-6
2-bromo-1-methoxy-3-nitrobenzene

: 17336-66-2
propiophenone N-tosylhydrazone

: 4-methoxy-2-methyl-3-phenyl-1H-indole

Guidance literature:: 2-bromo-1-methoxy-3-nitrobenzene; propiophenone N-tosylhydrazone; With bis-triphenylphosphine-palladium(II) chloride; lithium tert-butoxide; In 1,4-dioxane; at 100 ℃; for 7h; Inert atmosphere;

With carbon monoxide; 1,3-bis-(diphenylphosphino)propane; In 1,4-dioxane; at 140 ℃; for 72h; under 4560.31 Torr; Inert atmosphere;
DOI:10.1016/j.tet.2021.132331