(4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

Base Information

Chemical Name:(4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol
CAS No.:290293-82-2
Molecular Formula:C₂₇H₃₄O₂
Molecular Weight:390.566
Hs Code.:

Synonyms:(4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

Suppliers and Price of (4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

There total 5 articles about (4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: pseudopterosin U

: 100-39-0
benzyl bromide

: 290293-82-2
(4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

Guidance literature:: With potassium carbonate; In acetone; for 5h; Heating;
DOI:10.1021/np049802o

Reference yield: 90.0%

: 100-39-0
benzyl bromide

: pseudopterosin P

: 290293-82-2
(4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

Guidance literature:: With potassium carbonate; In acetone; for 5h; Heating;
DOI:10.1021/np049802o

Reference yield:

: Methanesulfonic acid (6S,6aR,9S)-1-benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-yl ester

: 290293-82-2
(4S,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

: (4R,6S,6aR,9S)-1-Benzyloxy-3,6,9-trimethyl-4-(2-methyl-propenyl)-5,6,6a,7,8,9-hexahydro-4H-phenalen-2-ol

Guidance literature:: With methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 18h; Yield given; Title compound not separated from byproducts;
DOI:10.1021/ja983041s