2-methylene-cyclopropanecarboxylic acid phenylamide

Base Information

Chemical Name:2-methylene-cyclopropanecarboxylic acid phenylamide
CAS No.:440084-62-8
Molecular Formula:C₁₁H₁₁NO
Molecular Weight:173.214
Hs Code.:

Synonyms:2-methylene-cyclopropanecarboxylic acid phenylamide

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Chemical Property of 2-methylene-cyclopropanecarboxylic acid phenylamide

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Technology Process of 2-methylene-cyclopropanecarboxylic acid phenylamide

There total 3 articles about 2-methylene-cyclopropanecarboxylic acid phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 62266-36-8
(+/-)-methylenecyclopropanecarboxylic acid

: 62-53-3
aniline

: 440084-62-8
2-methylene-cyclopropanecarboxylic acid phenylamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/ja011110o

Reference yield:

: 18941-94-1
2-methylene-cyclopropanecarboxylic acid ethyl ester

: 440084-62-8
2-methylene-cyclopropanecarboxylic acid phenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / K₂CO₃ / methanol; H₂O

2: 78 percent / EDCI / DMAP / CH₂Cl₂ / 5 h / 20 °C

With potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; In methanol; dichloromethane; water;
DOI:10.1021/ja011110o

Reference yield:

: 89892-99-9
2-bromo-2-methyl-cyclopropanecarboxylic acid ethyl ester

: 440084-62-8
2-methylene-cyclopropanecarboxylic acid phenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaH / diethyl ether

2: 91 percent / K₂CO₃ / methanol; H₂O

3: 78 percent / EDCI / DMAP / CH₂Cl₂ / 5 h / 20 °C

With sodium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/ja011110o