Technology Process of C22H17Br3ClN7O4
There total 6 articles about C22H17Br3ClN7O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
o-tetrachloroquinone;
copper(l) iodide; toluene-4-sulfonic acid;
In
1,4-dioxane;
for 6h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: caesium carbonate / N,N-dimethyl-formamide / 8 h / 100 °C
2: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / -78 - 20 °C
3: o-tetrachloroquinone / copper(l) iodide; toluene-4-sulfonic acid / 1,4-dioxane / 6 h / Inert atmosphere; Reflux
With
o-tetrachloroquinone; caesium carbonate; lithium diisopropyl amide;
copper(l) iodide; toluene-4-sulfonic acid;
In
tetrahydrofuran; 1,4-dioxane; n-heptane; ethylbenzene; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / -78 - 20 °C
2: o-tetrachloroquinone / copper(l) iodide; toluene-4-sulfonic acid / 1,4-dioxane / 6 h / Inert atmosphere; Reflux
With
o-tetrachloroquinone; lithium diisopropyl amide;
copper(l) iodide; toluene-4-sulfonic acid;
In
tetrahydrofuran; 1,4-dioxane; n-heptane; ethylbenzene;