dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate

Base Information

Chemical Name:dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate
CAS No.:1347661-62-4
Molecular Formula:C₂₄H₂₁NO₄
Molecular Weight:387.435
Hs Code.:

Synonyms:dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate

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Chemical Property of dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate

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Technology Process of dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate

There total 4 articles about dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1347661-60-2
3-(buta-1,3-dien-2-yl)-2-phenyl-1H-indole

: 762-42-5
dimethyl acetylenedicarboxylate

: 1347661-62-4
dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate

Guidance literature:: In dichloromethane; at 20 ℃; for 120h; Inert atmosphere; Darkness;
DOI:10.1016/j.tetlet.2011.10.003

Reference yield:

: 1347661-58-8
C₂₀H₁₈BrNO₂

: 1347661-62-4
dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 66 °C / Inert atmosphere

2: dichloromethane / 120 h / 20 °C / Inert atmosphere; Darkness

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.10.003

Reference yield:

: 116525-60-1
methyl (2-(phenylethynyl)phenyl)carbamate

: 1347661-62-4
dimethyl 4-(2-phenyl-1H-indol-3-yl)cyclohexa-1,4-diene-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro bis(acetonitrile) palladium(II); methyloxirane / tetrahydrofuran / 5 h / 25 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 66 °C / Inert atmosphere

3: dichloromethane / 120 h / 20 °C / Inert atmosphere; Darkness

With dichloro bis(acetonitrile) palladium(II); tetrabutyl ammonium fluoride; methyloxirane; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.10.003