C₁₆H₁₉NO₇

Base Information

Chemical Name:C₁₆H₁₉NO₇
CAS No.:946428-56-4
Molecular Formula:C₁₆H₁₉NO₇
Molecular Weight:337.329
Hs Code.:

C<sub>16</sub>H<sub>19</sub>NO<sub>7</sub>

Synonyms:C₁₆H₁₉NO₇

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Chemical Property of C₁₆H₁₉NO₇

Chemical Property:

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Technology Process of C₁₆H₁₉NO₇

There total 8 articles about C₁₆H₁₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 946428-55-3
C₂₂H₂₉NO₉

: 946428-56-4
C₁₆H₁₉NO₇

Guidance literature:: With hydrogenchloride; at 80 ℃; for 12h;
DOI:10.1021/ol070980t

Reference yield:

: N-carbomethoxy-L-3-dehydroproline methyl ester

: 946428-56-4
C₁₆H₁₉NO₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: aq. AcOH / Pd(OAc)2 / acetonitrile / 4 h / 60 °C

1.2: 65 percent / 2,4-lutidine; trifluoroacetic anhydride / toluene

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 79 percent / tetrahydrofuran

3.1: LiHMDS / tetrahydrofuran / 0.5 h / 0 °C

3.2: 72 percent / tetrahydrofuran / 18 h / 0 - 20 °C

4.1: H₂O₂ / tetrahydrofuran / 0 - 20 °C

5.1: H₂ / PtO₂ / ethanol / 3620.13 Torr

6.1: 80 percent / aq. HCl / 12 h / 80 °C

With hydrogenchloride; hydrogen; dihydrogen peroxide; sodium hydride; acetic acid; lithium hexamethyldisilazane; platinum(IV) oxide; palladium diacetate; In tetrahydrofuran; ethanol; acetonitrile; 2.2: Michael reaction;
DOI:10.1021/ol070980t

Reference yield:

: 492-95-5
2-methoxyphenyldiazonium tetrafluoroborate

: 946428-56-4
C₁₆H₁₉NO₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: aq. AcOH / Pd(OAc)2 / acetonitrile / 4 h / 60 °C

1.2: 65 percent / 2,4-lutidine; trifluoroacetic anhydride / toluene

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 79 percent / tetrahydrofuran

3.1: LiHMDS / tetrahydrofuran / 0.5 h / 0 °C

3.2: 72 percent / tetrahydrofuran / 18 h / 0 - 20 °C

4.1: H₂O₂ / tetrahydrofuran / 0 - 20 °C

5.1: H₂ / PtO₂ / ethanol / 3620.13 Torr

6.1: 80 percent / aq. HCl / 12 h / 80 °C

With hydrogenchloride; hydrogen; dihydrogen peroxide; sodium hydride; acetic acid; lithium hexamethyldisilazane; platinum(IV) oxide; palladium diacetate; In tetrahydrofuran; ethanol; acetonitrile; 2.2: Michael reaction;
DOI:10.1021/ol070980t