1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea

Base Information

Chemical Name:1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea
CAS No.:188436-79-5
Molecular Formula:C₂₁H₂₄ClN₃S
Molecular Weight:385.961
Hs Code.:

Synonyms:1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea

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Chemical Property of 1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea

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Technology Process of 1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea

There total 3 articles about 1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 173202-88-5
N-(2-chloromethylphenyl)benzimidoyl isothioxyanate

: 188436-79-5
1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea

Guidance literature:: In acetone; for 24h; Ambient temperature;
DOI:10.1135/cccc19961681

Reference yield:

: 19053-49-7
N-(2-tolyl)benzimidoyl chloride

: 188436-79-5
1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / SOCl₂, AIBN / benzene / 4 h / Heating

2: 70 percent / acetone / 1 h / -5 °C

3: 52 percent / acetone / 24 h / Ambient temperature

With thionyl chloride; 2,2'-azobis(isobutyronitrile); In acetone; benzene;
DOI:10.1135/cccc19961681

Reference yield:

: 168412-14-4
N-(2-chloromethylphenyl)benzimidoyl chloride

: 188436-79-5
1-{[(Z)-2-Chloromethyl-phenylimino]-phenyl-methyl}-3-cyclohexyl-thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / acetone / 1 h / -5 °C

2: 52 percent / acetone / 24 h / Ambient temperature

In acetone;
DOI:10.1135/cccc19961681