3,5-dimethyl-4-mercaptophenoxyacetic acid

Base Information

• Chemical Name: 3,5-dimethyl-4-mercaptophenoxyacetic acid
• CAS No.: 99186-49-9
• Molecular Formula: C₁₀H₁₂O₃S
• Molecular Weight: 212.269

Synonyms:3,5-dimethyl-4-mercaptophenoxyacetic acid

Chemical Property of 3,5-dimethyl-4-mercaptophenoxyacetic acid

Chemical Property:

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Technology Process of 3,5-dimethyl-4-mercaptophenoxyacetic acid

There total 1 articles about 3,5-dimethyl-4-mercaptophenoxyacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-chlorosulfonyl-3,5-dimethyl-phenoxy)-acetic acid ethyl ester (100389-06-8) → 3,5-dimethyl-4-mercaptophenoxyacetic acid (99186-49-9)

Guidance literature:

With amalgamated zinc; sulfuric acid;

DOI:10.1021/jo01116a602

Reference yield: 88.0%

5-chloro-1-methyl-4-nitroimidazole (4897-25-0) + 3,5-dimethyl-4-mercaptophenoxyacetic acid (99186-49-9) → 4-carboxymethoxy-2,6-dimethylphenyl 1-methyl-4-nitro-5-imidazolyl sulfide (135216-92-1)

Guidance literature:

With ammonia; In ethanol; a) 50 deg C, b) room temp., 3 h;

DOI:10.1002/jhet.5570280307

Reference yield: 82.0%

3,5-dimethyl-4-mercaptophenoxyacetic acid (99186-49-9) + 1-neopentyl-2-tert-butyl-4-nitro-5-chloroimidazole (135217-01-5) → 4-carboxymethoxy-2,6-dimethylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide (135217-02-6)

Guidance literature:

With ammonia; In ethanol; a) 50 deg C, b) room temp., 2 h;

DOI:10.1002/jhet.5570280307

upstream raw materials:

(4-chlorosulfonyl-3,5-dimethyl-phenoxy)-acetic acid ethyl ester

Downstream raw materials:

(4-mercapto-3,5-dimethyl-phenoxy)-acetic acid ethyl ester

bis-(4-carboxymethoxy-2,6-dimethyl-phenyl)-disulfide

4-carboxymethoxy-2,6-dimethylphenyl 1-methyl-4-nitro-5-imidazolyl sulfide

4-carboxymethoxy-2,6-dimethylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

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