2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)

Base Information

Chemical Name:2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)
CAS No.:120475-63-0
Molecular Formula:C₂₄H₂₂O₁₂
Molecular Weight:502.431
Hs Code.:

Synonyms:2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)

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Chemical Property of 2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)

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Technology Process of 2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)

There total 6 articles about 2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 120475-74-3
2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

: 120475-63-0
2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; for 0.416667h; Ambient temperature;
DOI:10.1021/jm00127a039

Reference yield:

: 120475-77-6
(Z)-1,2-bis<4-(acetoxymethyl)-2,5-dimethoxyphenyl>ethene

: 120475-63-0
2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / H₂ / PtO₂ / acetic acid / 6 h / 2068.6 Torr

2: 82 percent / NaOH / methanol; tetrahydrofuran; H₂O / Ambient temperature

3: 87 percent / Et₃N, 4-(dimethylamino)pyridine / dioxane / 24 h / Ambient temperature

4: 68 percent / Ce(NH₄)2(NO₃)6 / acetonitrile; H₂O / 0.42 h / Ambient temperature

With dmap; sodium hydroxide; ammonium cerium(IV) nitrate; hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; 1,4-dioxane; methanol; water; acetic acid; acetonitrile;
DOI:10.1021/jm00127a039

Reference yield:

: 20306-76-7
2,5,2',5'-tetramethoxy-bibenzyl

: 120475-63-0
2,2'-ethylenebis[5-(hydroxymethyl)-1,4-benzoquinone]bis(hydrogen succinate)

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / HCl-gas, conc. HCl / dioxane / 0.02 h

2: 81 percent / Na₂CO₃ / dioxane; H₂O / 8 h / Heating

3: 87 percent / Et₃N, 4-(dimethylamino)pyridine / dioxane / 24 h / Ambient temperature

4: 68 percent / Ce(NH₄)2(NO₃)6 / acetonitrile; H₂O / 0.42 h / Ambient temperature

With hydrogenchloride; dmap; ammonium cerium(IV) nitrate; sodium carbonate; triethylamine; In 1,4-dioxane; water; acetonitrile;
DOI:10.1021/jm00127a039